Society for Engineers of COMSATS (SECOM) organized MATLAB Workshop on the topic of “Numerical Computations and Optimization Techniques” on 18th May, 2016. This is the Phase-III Workshop organized by Society for Engineers of COMSATS (SECOM). MATLAB is the language of Technical computing. MATLAB platform is optimized for solving scientific problems. In this session, MATLAB and Optimization Toolbox for solving numerical computation problems had been introduced. It included a section on using Optimization Toolbox for determining Critical Points using various algorithms built in MATLAB. From this session, the students learnt MATLAB, Matrices operations, Root finding Techniques, Area finding techniques and Optimization techniques using OPTIMTOOL.